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In the presence of diastereoisomers, double peaks are sometimes recorded. In this case the sum of the two peaks is taken into account. In our laboratory, saturation shake- ask solubility is routinely performed at pH 6.8 and pH 1.0 (for acids only) 0.5 mL of buffer is added to about 2 mg of sample in a small borosilicate vial (2 mL) and sonicated for 3 minutes using a sonicating bath. The suspension is then incubated at 25.0 C for 20 hours in a thermostated water bath at a shaking speed of 200 cycles/min.The phases are separated by decantation/centrifugation.The supernatant is carefully collected and the solute quanti ed using the analytical method de ned previously. Before each injection, a blank is performed to avoid phantom peaks due to carryover or impurities present in the system. 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